I love this story and I have to give credit to Howard Mackie’s run during Volume 2 for introducing me to it.
Amazing Spider-Man (Vol. 1) #25
Published: c. April, 1965?
Cover Date: June, 1965
“Captured by J. Jonah Jameson!”
Plot: Steve Ditko
Script: Stan Lee
Artist: Steve Ditko
Inker: Steve Ditko
Letterer: Sam Rosen